Facile Synthesis of Tuneable Azophosphonium Salts

Open Access
Authors
Publication date 31-03-2019
Journal European Journal of Inorganic Chemistry
Volume | Issue number 2019 | 11-12
Pages (from-to) 1594-1603
Number of pages 10
Organisations
  • Faculty of Science (FNWI) - Van 't Hoff Institute for Molecular Sciences (HIMS)
Abstract Azophosphonium salts have a facile synthesis and can be readily tuned at the para position of the aryl group and at the phosphorus position with the use of bulky phosphines, leading to a range of coloured compounds. A relation between the Hammett σ+para constant and the colour and 31P NMR chemical shift was explored. The compounds were characterised by NMR spectroscopy, UV/Vis spectroscopy and single‐crystal X‐ray structure crystallography.
Document type Article
Note -In Special Issue: Phosphorus Chemistry. - With supplementary file
Language English
Related dataset CCDC 1866249: Experimental Crystal Structure Determination CCDC 1866248: Experimental Crystal Structure Determination CCDC 1866247: Experimental Crystal Structure Determination
Published at https://doi.org/10.1002/ejic.201801546
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ejic.201801546 (Final published version)
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