- Structure of tetrakis(melaminium) bis(dihydrogenphosphate) monohydrogenphosphate trihydrate from X-ray powder diffraction and solid-state NMR spectroscopy
- The Journal of Physical Chemistry. C
- Volume | Issue number
- 112 | 32
- Pages (from-to)
- Document type
- Faculty of Science (FNWI)
- Van 't Hoff Institute for Molecular Sciences (HIMS)
The crystal structure of the melamine phosphate salt tetrakis(melaminium) bis(dihydrogenphosphate) monohydrogenphosphate trihydrate with as much as ten independent moieties in the unit cell was determined by a direct-space global optimization technique from X-ray powder diffraction data using additional geometry constraints obtained by 31P double-quantum solid-state NMR spectroscopy. The structure analysis of the compound and its comparison with other melamine phosphates reveals the packing and bonding characteristics that are important for melamine-phosphate salts with a melamine-to-phosphor ratio larger than one, which are promising environmental-friendly flame retardants.
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