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Zoekopdracht: faculteit: "FNWI" en publicatiejaar: "2010"

AuteursC.F. Fu, C.C. Lee, Y.H. Liu, S.M. Peng, S. Warsink, C.J. Elsevier, J.T. Chen, S.T. Liu
TitelBiscarbene palladium(II) complexes. Reactivity of saturated versus unsaturated N-heterocyclic carbenes
TijdschriftInorganic Chemistry
Jaargang49
Jaar2010
Nummer6
Pagina's3011-3018
ISSN00201669
FaculteitFaculteit der Natuurwetenschappen, Wiskunde en Informatica
Instituut/afd.FNWI: Van 't Hoff Institute for Molecular Sciences (HIMS)
SamenvattingA series of designed palladium biscarbene complexes including saturated and unsaturated N-heterocyclic carbene (NHC) moieties have been prepared by the carbene transfer methods. All of these complexes have been characterized by 1H and 13C NMR spectroscopy as well as X-ray diffraction analysis. The reactivity of Pd−C(saturated NHC) is distinct from that of Pd−C(unsaturated NHC). The Pd−C(saturated NHC) bonds are fairly stable toward reagents such as CF3COOH, AgBF4 and I2, whereas Pd−C(unsaturated NHC) bonds are readily cleaved under the similar conditions. Notably, the catalytically activity of these palladium complexes on Suzuki−Miyaura coupling follows the order: (sat-NHC)2PdCl2 > (sat-NHC)(unsat-NHC)PdCl2 > (unsat-NHC)2PdCl2.
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